© Benaki Phytopathological Institute
Anagnostopoulos
et al.
86
lished at the time of analysis by the Europe-
an Union or FAO. The quantification of the
analytes was conducted by single-level cali-
bration. Single-level calibrationmay provide
Table 4 (continued)
Compound
1
st
level
(0.01 mg/kg)
2
nd
level
(0.05 mg/kg)
3
th
level
(0.5 mg/kg)
Mean
recovery
(%)
RSD
Mean
recovery
(%)
RSD
Mean
recovery
(%)
RSD
fenamidone
95.57
14.06
84.8
17.2
97.9
4.4
fenbuconazole
95.71
10.78
101.3
14.1
78.8
8.7
fenhexamid
96.77
19.44
111.0
6.4
92.0
6.8
fenoxycarb
121.22
5.26
110.4
13.6
77.3
9.6
fenpyroximate
125.29
8.19
119.7
26.9
92.2
26.8
fenthion
116.83
5.94
74.4
16.1
70.0
11.6
fosthiazate
105.32
15.58
98.6
3.6
109.4
1.7
hexaconazole
-
-
112.2
11.5
-
-
imidacloprid
103.94
20.09
96.1
4.8
103.7
3.0
indoxacarb
102.80
3.58
119.3
12.3
98.2
25.0
iprovalicarb
65.71
13.97
103.9
4.5
105.0
3.4
mepanipyrim
-
-
110.3
4.8
70.0
10.8
methiocarb
69.63
17.09
87.7
4.5
90.7
4.1
methiocarb sulfone
-
-
110.8
1.8
108.5
1.7
methiocarb sulfoxide
-
-
91.8
4.3
98.0
4.0
methomyl
119.57
19.78
75.4
18.8
95.3
2.1
methoxyfenozide
104.56
4.27
103.0
5.7
104.0
2.9
monocrotophos
116.64
17.56
70.4
6.3
71.9
3.8
myclobutanil
117.91
12.59
91.5
3.8
100.7
4.4
oxamyl
108.00
4.36
80.5
6.0
80.0
4.7
prochloraz
121.35
7.52
106.6
14.6
104.2
27.1
profenofos
119.92
19.64
105.1
18.3
74.0
12.9
pyraclostrobin
121.03
10.85
101.2
14.1
81.1
18.4
pyrimethanil
-
-
88.4
10.2
71.1
7.1
quinoxyfen
111.99
13.04
115.2
19.0
93.7
21.9
spinosad (A)
80.03
18.84
72.8
21.7
71.1
10.6
spiroxamine
123.87
17.23
79.4
10.6
81.5
7.0
tebuconazole
-
-
109.3
11.6
77.4
10.2
tebufenozid
113.83
12.2
101.7
5.3
98.3
5.2
tebufenpyrad
121.15
18.66
111.0
16.7
98.3
26.8
tetraconazole
108.22
24.68
89.8
13.4
80.3
7.4
thiabendazole
-
-
89.3
8.3
73.3
5.5
thiacloprid
122.85
9.31
70.0
19.8
94.3
2.5
thiamethoxam
123.39
20.66
92.6
6.4
91.2
3.1
thiodicarb
97.01
14.76
100.8
4.9
104.2
3.9
triadimefon
116.00
14.35
95.8
7.1
99.8
4.0
triadimenol
102.75
11.42
100.3
9.3
102.9
3.2
trifloxystrobin
101.77
8.62
76.8
20.7
72.3
13.7
vamidothion
94.71
11.44
75.3
6.9
87.9
1.3
1...,30,31,32,33,34,35,36,37,38,39 41,42,43,44,45,46,47,48,49,50,...65